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HRID647888

反应详情

EQUATION

反应方程式

HRID 647888 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：CCOC(=O)C(N)CCc1ccccc1
HCID4646380

未命名化合物

结构：CCOC(=O)CN1C(=O)C(Br)CCc2ccccc21
HCID13339963

Ethyl 3-bromo-2,3,4,5-tetrahydro-2-oxo-1H-1-benzazepine-1-acetate

C14H16BrNO3

PRODUCTS

生成物

1
结构：CCOC(=O)CN1C(=O)C(NC(CCc2ccccc2)C(=O)OCC)CCc2ccccc21
HCID13243517

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

Ethyl 2-amino-4-phenylbutyrate is treated in the presence of potassium carbonate in methylene chloride with 3-bromo-1-ethoxycarbonylmethyl-2,3,4,5-tetrahydro-1H-[1]benzazepin-2-one to give 1-ethoxycarbonylmethyl-3-(1-ethoxycarbonyl-3-phenylpropylamino)-2,3,4,5-tetrahydro-1H[1]benzazepin-2-one of example 10.