HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 20484309, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 20484284 | HCID 20484284 | — |
| Solvent | Hexamethylphosphoramide | HCID 12679 | — |
| Product | HCID 20484309 | HCID 20484309 | — |
Reaction Steps
The compound is formed analogously to that described in Example 28, from 3.3 g of 9-benzyl-1-methyl-7,8,9,10-tetrahydrothieno[3,2-e]pyrido[4,3-b]indole and 2 ml of benzyl bromide in 50 ml of hexamethylphosphoric acid triamide in the presence of NaH. Melting point: 206° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04410536 |
| Source dataset | uspto-grants-1983_10 |
| ORD ID | ord-accb3025a1394a01abfec8a12352de68 |
| Source note | uspto-grants-1983_10 |