HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20484156, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 13487077 | HCID 13487077 | — |
| Solvent | Isoamyl Alcohol | HCID 31260 | — |
| Product | HCID 20484156 | HCID 20484156 | — |
Reaction Steps
A solution of 283 mg. of 3-p-toluoyl-5,6,7,8-tetrahydropyrrolo[1,2-a]pyridine-8-carboxylic acid in 20 ml. of isoamyl alcohol is saturated with hydrogen chloride. After 24 hours, the excess alcohol is distilled off in vacuo and the residue purified by chromatography on alumina, to yield isoamyl 3-p-toluoyl-5,6,7,8-tetrahydropyrrolo[1,2-a]pyridine-8-carboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04410534 |
| Source dataset | uspto-grants-1983_10 |
| ORD ID | ord-cbe3219504104f468cd47c1fe510a77c |
| Source note | uspto-grants-1983_10 |