HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 23715406, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 13487077 | HCID 13487077 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 23715406 | HCID 23715406 | — |
Reaction Steps
To a solution of 283 mg. of 3-p-toluoyl-5,6,7,8-tetrahydropyrrolo[1,2-a]pyridine-8-carboxylic acid in 10 ml. of methanol is added 1 molar equivalent of sodium hydroxide, in the form of a 0.1 N solution. The solvent is then evaporated under reduced pressure and the residue taken up in 2 ml. of methanol, followed by precipitation with ether, to yield crude sodium 3-p-toluoyl-5,6,7,8-tetrahydropyrrolo[1,2-a]pyridine-8-carboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04410534 |
| Source dataset | uspto-grants-1983_10 |
| ORD ID | ord-8007df1e69014459a1c7509714c3e22f |
| Source note | uspto-grants-1983_10 |