HCID 20484852, compound → HCID 20484847, compound

Participants

Reaction Steps

350 mg of the product of Step D were dissolved in 100 ml of ethyl acetate and an inert gas was bubbled therethrough for 15 minutes and the solution was then irridated with a mercury vapor lamp. After 10 minutes, 33 ml of nitrogen were disengaged and the solution was evaporated to dryness to obtain 290 mg of ethyl 3,3-dimethyl-2-(2-hydroxy-2-methyl-propyl)-cyclopropane-1-carboxylate.

Provenance & Evidence