Benzaldehyde → HCID 13806364, compound

Participants

Reaction Steps

Using diphenylaminoborane dichloride (200 mg), benzaldehyde (85 mg) and tri-n-butylamine (147 mg), the reaction is effected as in Example 7, whereby 2-phenylaminobenzhydrol (49 mg) is obtained. This substance is recrystallized from benzene-hexane to give crystals melting at 111° to 112° C. Anal. Calcd. for C19H17ON: C, 82.88; H, 6.62; N, 5.09. Found: C, 82.67; H, 6.28; N, 5.03.

Provenance & Evidence