Hydrogen Peroxide → N,N-Dimethylheptan-1-amine N-oxide

HRID 648176Notes

Reaction equation

[CH3:1][N:2]([CH3:10])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9].[OH:11]O>>[CH3:1][N+:2]([O-:11])([CH3:10])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9]

Participants

Reactant 2

HCID 784Hydrogen Peroxide

HCID 16226N,N-Dimethylheptylamine

Product 1

HCID 5189203N,N-Dimethylheptan-1-amine N-oxide

Procedure

To 28.6 g of dimethylheptyl amine was added slowly 100 ml 30% H2O2 as in Example 4 to give the dimethylheptyl amine oxide. NMR showed the resulting semisolid material to contain 29% water and 71% of the amine oxide.

Sources & evidence

ORD record: ord-752520db35a84cba98bc9968885876b5
Source dataset: uspto-grants-1983_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04411893

Reaction notes

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