HCID 20482366, compound → HCID 20482357, compound

HRID 648184Notes

Reaction equation

HRID 648184 reaction equation
Br[CH2:2][CH:3]([OH:16])[CH2:4][O:5][C:6]1[S:7][C:8]([C:11](=[O:15])[N:12]([CH3:14])[CH3:13])=[CH:9][N:10]=1.[C:17]1(=[O:27])[NH:21][C:20](=[O:22])[C:19]2=[CH:23][CH:24]=[CH:25][CH:26]=[C:18]12.[K]>CN(C)C=O>[C:17]1(=[O:27])[N:21]([CH2:2][CH:3]([OH:16])[CH2:4][O:5][C:6]2[S:7][C:8]([C:11](=[O:15])[N:12]([CH3:14])[CH3:13])=[CH:9][N:10]=2)[C:20](=[O:22])[C:19]2=[CH:23][CH:24]=[CH:25][CH:26]=[C:18]12

Participants

4

Reactant 2

HCID 20482366HCID 20482366, compoundHCID 24194345Phthalimide potassium salt

Product 1

HCID 20482357HCID 20482357, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

By a procedure analogous to Example 2 the product from Example 7 can be reacted with potassium phthalimide in N,N-dimethylformamide to give the solid title compound.

Sources & evidence

ORD record
ord-e96383820edd4325891aa98438abb5b2
Source dataset
uspto-grants-1983_10
Patent number
US04411899

Reaction notes

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