Hydrazine → HCID 20482388, compound

Participants

Reaction Steps

The product from Example 9 (4.0 g, 10.6 mmol) can be added to a solution of hydrazine (0.38 g, 12 mmol) in absolute ethanol (20 ml) and the suspension refluxed 4 hours under nitrogen on a steam bath. The mixture can then be cooled and filtered and the filtrate concentrated in vacuo to give the title compound as an oil.

Provenance & Evidence