HuagongsheHuagongshe Chemistry Print Report · For research reference only
Epichlorohydrin → HCID 12784476, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Epichlorohydrin | HCID 7835 | — |
| Reactant | HCID 12784475 | HCID 12784475 | — |
| Catalyst | Piperidine | HCID 8082 | — |
| Product | HCID 12784476 | HCID 12784476 | — |
Reaction Steps
Two drops of piperidine are added to 1.8 g 6,7,8,9-tetrahydro-7,7-dimethyl-6-oxo-5H-benzocyclohepten-1-ol in 8 ml epichlorohydrin. The mixture is stirred at 100° for 4 hours. The solution is evaporated, taken up in ether, filtered and concentrated to give crude 1-(3-chloro-2-hydroxypropoxy)-6,7,8,9-tetrahydro-7,7-dimethyl-5H-benzocyclohepten-6-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04411913 |
| Source dataset | uspto-grants-1983_10 |
| ORD ID | ord-ef0a1fb9c9014169b13b8348ae0d4bd6 |
| Source note | uspto-grants-1983_10 |