反应详情

A 1000 ml resin kettle was equipped with a still head, air bubbler, and thermometer. The kettle was placed in a regulated water bath, set at 80°. 750 ml methyl methacrylate was added to the kettle followed by a solution containing 250 g morpholinoethanol, 5.0 g sodium methoxide and 0.5 g p-methoxyphenol. During the 120 minute reaction time, air was bubbled slowly through the vigorously stirred solution. After 30 and 60 minutes, 5.0 g sodium methoxide was added. At the end of the reaction time, the mixture was cooled and neutralized with 17.0 g glacial acetic acid.

1. customThe kettle was placed in a regulated water bath
2. customset at 80°
3. customDuring the 120 minute reaction time, air
4. customwas bubbled slowly through the vigorously stirred solution
5. additionAfter 30 and 60 minutes, 5.0 g sodium methoxide was added
6. temperatureAt the end of the reaction time, the mixture was cooled