反应详情

To a stirred mixture of 1.26 g of 1H-1,2,4-triazole-1-propanamine in 30 ml of dichloromethane containing an excess of saturated sodium bicarbonate solution was added, all at once at room temperature, a solution of 1.27 ml of benzenesulfonyl chloride in 15 ml of dichloromethane. The mixture was stirred at room temperature for 16 hours. The layers were separated. The dichloromethane layer was evaporated in vacuo and gave the compound of the Example as a colorless oil.

1. additionwas added
2. customonce at room temperature
3. customThe layers were separated
4. customThe dichloromethane layer was evaporated in vacuo
5. customgave the compound of the Example as a colorless oil