Hexanoyl chloride → HCID 2058674, compound

HRID 648610Notes

Reaction equation

[NH2:1][C@@H:2]([C:4]([OH:6])=[O:5])[CH3:3].[C:7](Cl)(=[O:13])[CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]>>[C:7]([NH:1][C@H:2]([CH3:3])[C:4]([OH:6])=[O:5])(=[O:13])[CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Participants

Reactant 2

HCID 67340Hexanoyl chloride

HCID 71080D-Alanine

Product 1

HCID 2058674HCID 2058674, compound

Procedure

D-alanine (20 mmol) and hexanoyl chloride (22 mmol) were reacted using the method as described in Example 5 Part A to give the title compound as a white crystalline material (2.45 g, 65.5%) after recrystallization from isopropyl ether (20 ml), m.p. 82°-95° C.

Sources & evidence

ORD record: ord-9a3e63fc20c541cb824dd54288a8bf87
Source dataset: uspto-grants-1988_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04735962

Reaction notes

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