HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 20145110, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 20145227 | HCID 20145227 | — |
| Catalyst | Silver(II) oxide | HCID 92152 | — |
| Product | HCID 20145110 | HCID 20145110 | — |
Reaction Steps
The above compound was prepared from 4-[(1-(2-piperidinophenyl)-ethyl)-aminocarbonylmethyl]-benzaldehyde by heating with silver oxide in the presence of 1N sodium hydroxide solution for 20 minutes in a steam bath, subsequent acidification with 2N sulfuric acid at a pH of 5, extraction with ethyl acetate, and purification by column chromatography on silica gel (toluene/acetone=1:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04735959 |
| Source dataset | uspto-grants-1988_04 |
| ORD ID | ord-4c6d13faa57d42f8bb948ff0e46716dd |
| Source note | uspto-grants-1988_04 |