HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20145121, compound → HCID 20145110, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20145121 | HCID 20145121 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20145110 | HCID 20145110 | — |
Reaction Steps
One hundred milligrams (0.2744 m mol) of 4-[(1-(2-piperidino-phenyl)-ethenyl)-aminocarbonylmethyl]-benzoic acid in 5 ml of absolute ethanol were hydrogenated in the presence of 50 mg of palladium/charcoal (10%) at 20° C. and at a hydrogen pressure of 1 bar under shaking. After 1.5 hours the catalyst was filtered off, and the filtrate was evaporated in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04735959 |
| Source dataset | uspto-grants-1988_04 |
| ORD ID | ord-3e08ba48da064ac7b147909a50831d62 |
| Source note | uspto-grants-1988_04 |