Aluminium lithium hydride → HCID 57171140, compound

HRID 648634Notes

Reaction equation

HRID 648634 reaction equation
C([O:3][C:4](=O)[C:5]1[CH:10]=[CH:9][C:8]([CH:11]([CH:15]([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=2[N:23]2[CH2:28][CH2:27][CH2:26][CH2:25][CH2:24]2)[CH3:16])[C:12]([NH2:14])=[O:13])=[CH:7][CH:6]=1)C.[H-].[Al+3].[Li+].[H-].[H-].[H-]>O1CCCC1>[N:23]1([C:18]2[CH:19]=[CH:20][CH:21]=[CH:22][C:17]=2[CH:15]([CH:11]([C:12]([NH2:14])=[O:13])[C:8]2[CH:7]=[CH:6][C:5]([CH2:4][OH:3])=[CH:10][CH:9]=2)[CH3:16])[CH2:24][CH2:25][CH2:26][CH2:27][CH2:28]1

Participants

4

Reactant 2

HCID 21226445Aluminium lithium hydrideHCID 57127153HCID 57127153, compound

Product 1

HCID 57171140HCID 57171140, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

Prepared from 4-[(1-(2-piperidino-phenyl)-ethyl)-aminocarbonylmethyl]-benzoic acid ethyl ester by lithium aluminum hydride reduction in tetrahydrofuran.

Sources & evidence

ORD record
ord-52b9c29010f944428902b785d6ca64f8
Source dataset
uspto-grants-1988_04
Patent number
US04735959

Reaction notes

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