Acetic Anhydride → HCID 20145283, compound

Participants

Reaction Steps

An amount of 0.35 gm (0.915 m mol) of 4-[(1-(5-hydroxy-2-piperidinophenyl)-ethyl)-aminocarbonylmethyl]-benzoic acid was heated together with 0.103 ml (1.098 m mol) of acetic anhydride on a steam bath, and after standing for four days at 20° C., the reaction mixture was recrystallized from methanol.

Provenance & Evidence