HRID64868

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID7477

Benzoyl chloride, 4-methoxy-

C8H7ClO2

HCID100614

1-((Pyrrolidine-1-carbonyl)methyl)piperazine

C10H19N3O

PRODUCTS

生成物

结构：COc1ccc(C(=O)N2CCN(CC(=O)N3CCCC3)CC2)cc1.Cl

HCID13371229

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6344

Dichloromethane

CH2Cl2

2 次

CONDITIONS

反应条件

温度: 25 °C

PROCEDURE

实验过程

9.4 g of piperazin-1-yl-acetic acid pyrrolidide are dissolved in 10 ml of methylene chloride. A solution of 8.75 g of anisic acid chloride in 10 ml of methylene chloride is added dropwise at 0°. After the mixture had been stirred at 25° C. for 60 minutes, the crystals are filtered off with suction and dried in vacuo.

WORKUP

后处理

filtrationthe crystals are filtered off with suction
customdried in vacuo