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HRID64869

反应详情

EQUATION

反应方程式

HRID 64869 的结构方程式

REACTANTS

反应物

6
结构：C1CNCCN1
HCID4837

Piperazine

C4H10N2

结构：O=C(Cl)CCl
HCID6577

Chloroacetyl chloride

C2H2Cl2O

结构：COc1ccc(C(=O)Cl)cc1
HCID7477

Benzoyl chloride, 4-methoxy-

C8H7ClO2

结构：C1COCCN1
HCID8083

Morpholine

C4H9NO

结构：O=C(CCl)N1CCOCC1
HCID74040

2-Chloro-1-(morpholin-4-yl)ethanone

C6H10ClNO2

结构：COc1ccc(C(=O)N2CCNCC2)cc1
HCID2736724

1-(4-Methoxybenzoyl)-piperazine

C12H16N2O2

PRODUCTS

生成物

1
结构：COc1ccc(C(=O)N2CCN(CC(=O)N3CCOCC3)CC2)cc1
HCID779179

Molracetam

C18H25N3O4

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

结构：Cc1ccccc1
溶剂HCID1140

Toluene

C7H8

PROCEDURE

实验过程

The N-(4-methoxybenzoyl)-piperazine used as a starting substance was obtained as a viscous oil by reacting 1 mol of piperazine with 0.5 mol of anisic acid chloride in glacial acetic acid. The chloroacetic acid morpholide used as a starting substance was obtained as a colourless oil by reacting 2 mol of morpholine with 1 mol of chloroacetyl chloride in toluene.

WORKUP

后处理

  1. customwas obtained as a viscous oil
  2. customwas obtained as a colourless oil