HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Anisoyl chloride → HCID 70452558, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Anisoyl chloride | HCID 7477 | — |
| Reactant | N-isopropyl-1-piperazineacetamide | HCID 100826 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 70452558 | HCID 70452558 | — |
Reaction Steps
A solution of 4.6 g of anisic acid chloride in 20 ml of methylene chloride is added dropwise to 5 g of piperazinoacetic acid isopropylamide in 20 ml of methylene chloride at 0° C. The mixture is then stirred at room temperature for 4 hours and subsequently concentrated. The residue is recrystallised from isopropanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04610984 |
| Source dataset | uspto-grants-1986_09 |
| ORD ID | ord-8c3022f585c949368e9772787e8e09b8 |
| Source note | uspto-grants-1986_09 |