HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 3-Dimethylsilyl-5-methyl-2-oxazolidinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Chlorodimethylsilane | HCID 66108 | — |
| Reactant | 5-Methyl-2-oxazolidinone | HCID 136837 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 3-Dimethylsilyl-5-methyl-2-oxazolidinone | HCID 123340980 | — |
Reaction Steps
A 3-dimethylsilyl-5-methyl-2-oxazolidinone was prepared in accordance with the following procedure. A stirred mixture of 60.6 grams of 5-methyl-2-oxazolidinone and 62.4 grams of triethylamine was prepared in a tetrahydrofuran solvent. To this mixture, 67.5 ml of dimethylchlorosilane was added dropwise over a period of 90 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04736046 |
| Source dataset | uspto-grants-1988_04 |
| ORD ID | ord-5a21bbb0de154e27b3e4262db03f0ec1 |
| Source note | uspto-grants-1988_04 |