Hydrochloric Acid → HCID 54018226, compound

Participants

Reaction Steps

In the temperature range from -10° C. to 0° C. and with stirring, a solution of 7.55 g of p-chlorosulfonylbenzoic acid in 25 g of tetrahydrofuran is slowly added to a solution of 5 g of α-hydroxyiminobenzyl cyanide in 24 g of tetrahydrofuran. The reaction mixture is heated, with stirring, to room temperature. After 2 hours, the reaction mixture is poured into 600 ml of 0.12N hydrochloric acid. The precipitated product is isolated by filtration, washed with water and dried at 40° C. in vacuo. Melting point: 250°-251° C.

Provenance & Evidence