HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 13654955, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 20144154 | HCID 20144154 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13654955 | HCID 13654955 | 86.6% |
Reaction Steps
1.0 g of morpholine and 2.3 g of 2-methyl-1,3-dithiolium bromide were treated in the same manner as in Example 26, and the product was recrystallized from ethanol, whereby 2.2 g (yield: 86.6%) of 4-(1,3-dithiol-2-ylidene)morpholinium bromide (Compound No. 28) was obtained as crystals having a melting point of 274° to 276° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04737494 |
| Source dataset | uspto-grants-1988_04 |
| ORD ID | ord-a6dbf040adb24727875bae4388f7595b |
| Source note | uspto-grants-1988_04 |