HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Benzylpiperazine → HCID 13654959, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Benzylpiperazine | HCID 75994 | — |
| Reactant | 2-Methylthio-1,3-dithiolium perchlorate | HCID 23039009 | — |
| Product | HCID 13654959 | HCID 13654959 | 68.9% |
Reaction Steps
2.2 g of N-benzylpiperazine and 2.5 g of 2-methylthio-1,3-dithiolium perchlorate were treated in the same manner as in Example 26, and the product was recrystallized from water-ethanol, whereby 2.6 g (yield: 68.9%) of 1-(1,3-dithiol-2-ylidene)-4-benzylpiperazinium perchlorate (Compound No. 33) was obtained as crystals having a melting point of from 224° to 226° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04737494 |
| Source dataset | uspto-grants-1988_04 |
| ORD ID | ord-b23bbb5850b64d75a3628a1e1eceaf74 |
| Source note | uspto-grants-1988_04 |