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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 649066Generated: October 31, 2026

Potassium Carbonate → HCID 13490894, compound

https://huagongshe.com/reaction/649066

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantN-MethyloctadecylamineHCID 75539—
ReactantHCID 22837660HCID 22837660—
SolventDimethylformamideHCID 6228—
ProductHCID 13490894HCID 13490894—

Reaction Conditions

Temperature50 °C

Reaction Steps

3.1 g of the compound of Example 47 are dissolved in 50 ml of dimethylformamide and treated with 5.0 g of potassium carbonate. 1.8 g of N-methyloctadecylamine are added and the mixture is heated to 50° C. After the reaction has ended, the mixture is cooled to room temperature and filtered, the filtrate is evaporated in vacuo and the residue is purified by column chromatography (eluent toluene/isopropanol 10:1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04737488
Source datasetuspto-grants-1988_04
ORD IDord-17da0920942341d8b0fedf7e6a32fa20
Source noteuspto-grants-1988_04