HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 649066Generated: October 31, 2026
Potassium Carbonate → HCID 13490894, compound
https://huagongshe.com/reaction/649066
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | N-Methyloctadecylamine | HCID 75539 | — |
| Reactant | HCID 22837660 | HCID 22837660 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 13490894 | HCID 13490894 | — |
Reaction Steps
3.1 g of the compound of Example 47 are dissolved in 50 ml of dimethylformamide and treated with 5.0 g of potassium carbonate. 1.8 g of N-methyloctadecylamine are added and the mixture is heated to 50° C. After the reaction has ended, the mixture is cooled to room temperature and filtered, the filtrate is evaporated in vacuo and the residue is purified by column chromatography (eluent toluene/isopropanol 10:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04737488 |
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| Source dataset | uspto-grants-1988_04 |
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| ORD ID | ord-17da0920942341d8b0fedf7e6a32fa20 |
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| Source note | uspto-grants-1988_04 |
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