Methyl iodide → HCID 86742104, compound

Participants

Reaction Steps

Ethyl 2-{4-[(6-chloro-1-methylquinolin-3-yl)oxy]phenoxy}propionate iodide salt (8) was prepared by reacting a mixture of ethyl 2-{4-[(6-chloroquinolin-3-yl)oxy]phenoxy}propionate (see Example 7) and methyl iodide in dichloromethane at ambient temperature for a period of four days. The product, a viscous oil, was characterized by its proton magnetic resonance spectrum. Pmr spectrum (CDCl3 ; in ppm): 10.1 (1H, d); 8.8 (1H, d); 8.65 (1H, d); 8.5 (1H, d); 8.05 (1H, d of d); 7.3 (4H, d of d); 4.95 (4H, m); 4.25 (2H, q); 1.6 (3H, d); 1.2 (3H, t).

Provenance & Evidence