Ethanol → HCID 18605010, compound

HRID 649246Notes

Reaction equation

HRID 649246 reaction equation
[NH2:1][CH2:2][C:3]([OH:5])=[O:4].[NH2:6][OH:7].[CH2:8](O)C>>[OH:7][NH:6][C@H:2]([C:3]([OH:5])=[O:4])[CH3:8].[NH2:1][CH2:2][C:3]([OH:5])=[O:4]

Participants

4

Reactant 3

HCID 702EthanolHCID 750GlycineHCID 787Hydroxylamine

Product 1

HCID 18605010HCID 18605010, compound

Procedure

3 g of N-(R, 2-bromo propanoyl)-glycine obtained by condensation of 2-bromo propionic acid (prepared according to E. Fischer et al., Annalen, 357, 1 (1907) with the glycine are dissolved in 100 ml of anhydrous ethanol and stirred for 48 hours with anhydrous hydroxylamine according to Example 5.

Workup

  1. customprepared

Sources & evidence

ORD record
ord-c439763930ed423db26d732320605123
Source dataset
uspto-grants-1988_04
Patent number
US04738803

Reaction notes

Loading…