HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20142115, compound → HCID 20142156, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20142115 | HCID 20142115 | — |
| Reactant | Butanol acetic acid water | HCID 22056973 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetic acid methanol water | HCID 86607755 | — |
| Product | HCID 20142156 | HCID 20142156 | — |
Reaction Steps
127 mg of the compound of Example 31 are dissolved in 3 ml of the mixture CH3OH/AcOH/H2O, 4/5/1 and hydrogenated at ordinary pressure in the presence of 30 mg of 10% Pd/C. After 1 hour, the theoretical volume is absorbed or filtered, and concentrated to dryness giving a white solid. W 88 mg. Rdt 88%; Rf 0.85; BuOH/AcOH/H2O, 4/1/1/.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04738803 |
| Source dataset | uspto-grants-1988_04 |
| ORD ID | ord-251827cdf1a6422cab5575174169b718 |
| Source note | uspto-grants-1988_04 |