HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 14809493, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 14809492 | HCID 14809492 | — |
| Product | HCID 14809493 | HCID 14809493 | 85.3% |
Reaction Steps
A mixture of 2-chloro-3,4-dihydro-2-(2-hydroxy-5-methoxyphenyl)-4-methyl-3-oxo-2H-1,4-benzothiazine (14.0 g, compound No. 3) and methanol (200 ml) is stirred for 2 hours at room temperature, and the separated crystals are collected by filtration to give 11.8 g (85.3%) of the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04739050 |
| Source dataset | uspto-grants-1988_04 |
| ORD ID | ord-8dc0d765e6054906b9896044b16b1db3 |
| Source note | uspto-grants-1988_04 |