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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 649310Generated: October 31, 2026

Methanol → HCID 14809493, compound

https://huagongshe.com/reaction/649310

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantHCID 14809492HCID 14809492—
ProductHCID 14809493HCID 1480949385.3%

Reaction Steps

A mixture of 2-chloro-3,4-dihydro-2-(2-hydroxy-5-methoxyphenyl)-4-methyl-3-oxo-2H-1,4-benzothiazine (14.0 g, compound No. 3) and methanol (200 ml) is stirred for 2 hours at room temperature, and the separated crystals are collected by filtration to give 11.8 g (85.3%) of the titled compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04739050
Source datasetuspto-grants-1988_04
ORD IDord-8dc0d765e6054906b9896044b16b1db3
Source noteuspto-grants-1988_04