HRID64939

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID240

Benzaldehyde

C7H6O

HCID70370

2,6-Di-tert-butyl-4-mercaptophenol

C14H22OS

PRODUCTS

生成物

结构：CC(C)(C)c1cc(SC(Sc2cc(C(C)(C)C)c(O)c(C(C)(C)C)c2)c2ccccc2)cc(C(C)(C)C)c1O

HCID13710010

未命名化合物

收率 66.3%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

The procedure of Example 1 is repeated using 23.84 grams of 2,6-di-tert-butyl-4-mercaptophenol, 5.31 grams of benzaldehyde, and 150 ml of methyl alcohol. The product is triturated with methyl alcohol to give 18.74 grams (66% yield) of white crystals, mp 122°-124° C.

WORKUP

后处理

customThe product is triturated with methyl alcohol