huagongshe.com
HRID64941

反应详情

EQUATION

反应方程式

HRID 64941 的结构方程式

REACTANTS

反应物

2
结构：O=C1CCCCC1
HCID7967

Cyclohexanone

C6H10O

结构：CC(C)(C)c1cc(S)cc(C(C)(C)C)c1O
HCID70370

2,6-Di-tert-butyl-4-mercaptophenol

C14H22OS

PRODUCTS

生成物

1
结构：CC(C)(C)c1cc(SC2(Sc3cc(C(C)(C)C)c(O)c(C(C)(C)C)c3)CCCCC2)cc(C(C)(C)C)c1O
HCID13710012

未命名化合物

收率 93.3%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

The procedure of Example 1 was repeated using 28.71 grams of 2.6-di-tert-butyl-4-mercaptophenol, 5.91 grams of cyclohexanone, and 150 ml of methyl alcohol. The product is triturated with methyl alcohol to give 31.17 grams (93.3% yield) of white solid, mp 195°-197° C.

WORKUP

后处理

  1. customThe product is triturated with methyl alcohol