HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanone → HCID 13710012, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanone | HCID 7967 | — |
| Reactant | 2,6-Di-tert-butyl-4-mercaptophenol | HCID 70370 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 13710012 | HCID 13710012 | 93.3% |
Reaction Steps
The procedure of Example 1 was repeated using 28.71 grams of 2.6-di-tert-butyl-4-mercaptophenol, 5.91 grams of cyclohexanone, and 150 ml of methyl alcohol. The product is triturated with methyl alcohol to give 31.17 grams (93.3% yield) of white solid, mp 195°-197° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04611023 |
| Source dataset | uspto-grants-1986_09 |
| ORD ID | ord-49ac09a1bc5c4585ae64f08ade600ca0 |
| Source note | uspto-grants-1986_09 |