Diallylamine → HCID 14076562, compound

Participants

Reaction Conditions

Reaction Steps

10.5 g (0.05 mole) of 2-cyano-2-ethyl-2-phenylacetyl chloride are dissolved in 50 ml of dichloromethane, the solution is cooled to 5° C., and 9.7 g (0.01 mole) of diallyl amine are added to it under maintaining the temperature of the mixture below 10° C. The reaction mixture is stirred at room temperature for 2 hours, then washed with water, dried over anhydrous magnesium sulfate, and the solvent is removed. 8.79 g (65.5%) of N,N-diallyl-2-cyano-2-ethyl-2-phenylacetic acid amide are obtained; m.p.: 33°-35° C.

Provenance & Evidence