Methanol → HCID 20141318, compound

Participants

Reaction Steps

14.1 g of N-(4-chlorophenylsulfonyl)-dithiocarbamic acid-S-methyl ester (0.05 mol) are refluxed in 100 ml of methanol, and after about 5 hours the formation of mercaptan has finished. The solvent is distilled off in a rotary evaporator, and the residue is recrystallised from methanol; yield 116 g (87% of theory), m.p. 129°-130° C.

Provenance & Evidence