Hydrochloric Acid → HCID 57167807, compound

HRID 649616Notes

Reaction equation

HRID 649616 reaction equation
Cl.C([O:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[C:13]([C:19]1[NH:20][CH:21]=[CH:22][N:23]=1)=[CH:14][S:15][CH2:16][CH2:17][CH3:18])CCC>>[OH:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[C:13]([C:19]1[NH:23][CH:22]=[CH:21][N:20]=1)=[CH:14][S:15][CH2:16][CH2:17][CH3:18]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 57138139HCID 57138139, compound

Product 1

HCID 57167807HCID 57167807, compound

Procedure

After adding an equivalent amount of hydrogen chloride to 200 mg of an oily substance which was Isomer B of 1-(2-n-butyloxyphenyl)-1-imidazolyl-2-n-propylthioethylene obtained from Compound 19 in the same manner as in Example 6, the resultant precipitate was recrystallized from ethyl acetate/acetone to obtain 140 mg of Isomer B (Compound 21) of 1-(2-n-butyloxyphenyl)-1-imidazolyl-2-n-propylthioethylene hydrochloride as colorless crystals.

Sources & evidence

ORD record
ord-12771302da6b4254bd84233e53b27094
Source dataset
uspto-grants-1988_04
Patent number
US04740601

Reaction notes

Loading…