Hydrochloric Acid → HCID 57323911, compound

HRID 649619Notes

Reaction equation

HRID 649619 reaction equation
Cl.C([O:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[C:13]([C:22]1[NH:23][CH:24]=[CH:25][N:26]=1)=[CH:14][S:15][C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1)CCC>>[OH:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[C:13]([C:22]1[NH:26][CH:25]=[CH:24][N:23]=1)=[CH:14][S:15][C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 57140840HCID 57140840, compound2×

Product 1

HCID 57323911HCID 57323911, compound

Procedure

After adding an equivalent amount of hydrogen chloride to 100 mg of an oily substance which was Isomer B (Compound 66) of 1-(2-n-butyloxyphenyl)-1-imidazolyl-2-phenylthioethylene obtained from Compound 62 in the same manner as in Example 10, the resultant precipitate was recrystallized from ethyl acetate/acetone to obtain 75 mg of Isomer B (Compound 95) of 1-(2-n-butyloxyphenyl)-1-imidazolyl-2-phenylthioethylene hydrochloride as colorless crystals.

Sources & evidence

ORD record
ord-24f8e294eb56478f83d0b0b1782a40a8
Source dataset
uspto-grants-1988_04
Patent number
US04740601

Reaction notes

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