3-Amino-1-propanol → HCID 13750866, compound

HRID 649657Notes

Reaction equation

HRID 649657 reaction equation
[N+:1]([C:4]1[C:9]([N+:10]([O-])=O)=[CH:8][C:7]([OH:13])=[C:6]([O:14][CH3:15])[CH:5]=1)([O-:3])=[O:2].N[CH2:17][CH2:18][CH2:19][OH:20]>O>[OH:20][CH2:19][CH2:18][CH2:17][NH:10][C:9]1[C:4]([N+:1]([O-:3])=[O:2])=[CH:5][C:6]([O:14][CH3:15])=[C:7]([OH:13])[CH:8]=1

Participants

4

Reactant 2

HCID 90863-Amino-1-propanolHCID 184586Phenol, 2-methoxy-4,5-dinitro-

Product 1

HCID 13750866HCID 13750866, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

A mixture consisting of 0.2 mol (42.8 g) of 4,5-dinitro-2-methoxyphenol, prepared in Example 2, 0.6 mol (45.7 g) of 3-amino-1-propanol and 30 ml of water is heated at the refluxing temperature of water for 3 h 30 min.

Sources & evidence

ORD record
ord-b5249afcda2e4ece867b415a4ce9579d
Source dataset
uspto-grants-1988_04
Patent number
US04740622

Reaction notes

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