HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 649711Generated: October 30, 2026
Potassium Carbonate → HCID 18003869, compound
https://huagongshe.com/reaction/649711
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Benzene, 1-fluoro-2-methyl-4-nitro- | HCID 68001 | — |
| Reactant | 1H-Imidazole-1-propanamine | HCID 78736 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 18003869 | HCID 18003869 | — |
Reaction Steps
A mixture of 250.4 g (2 mol) of 3-imidazol-1-ylpropylamine and 82.8 g (0.6 mol) of potassium carbonate in 280 ml of water was heated to 90° C. 155.1 g (1 mol) of 1-fluoro-2-methyl-4-nitrobenzene were added dropwise over 30 minutes and the mixture was maintained at a temperature of 90-95° C. for 4 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06270533B1 |
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| Source dataset | uspto-grants-2001_08 |
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| ORD ID | ord-2c81e43639a8439d891969d2711a07e8 |
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| Source note | uspto-grants-2001_08 |
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