HRID649713

反应详情

EQUATION

反应方程式

HRID 649713 反应方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

54.5 g (0.2 mol) of N-[2-(3-chloropropoxy)-4-nitrophenyl]acetamide, the preparation of which was described in step a) of Example 6 above, and 40.8 g (0.6 mol) of 1H imidazole in 150 ml of dimethylformamide were heated on a boiling water bath for 4 hours.

WORKUP

后处理

  1. temperaturewere heated on a boiling water bath for 4 hours