HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10549647, compound → HCID 10779605, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10549647 | HCID 10549647 | — |
| Solvent | Ammonia methanol | HCID 21705897 | — |
| Product | HCID 10779605 | HCID 10779605 | 118.6% |
Reaction Steps
Compound 3(200 mg,0.5 mmol) was dissolved in saturated NH3/MeOH (5 mL) and stirred at room temperature for two hours. The solvent was evaporated in vacuo to obtain crude 4 (170 mg) which was used for the subsequent reaction without any further purification: UV (Me(OH)λmax 263.0 nm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06271212B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-50fd73e9599347668ef1404556623365 |
| Source note | uspto-grants-2001_08 |