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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 649939Generated: October 29, 2026

Anisole → HCID 135816406, compound

https://huagongshe.com/reaction/649939

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAnisoleHCID 7519—
Reactant1-MethylpiperazineHCID 53167—
ReactantHCID 18422381HCID 18422381—
CatalystTitanium TetrachlorideHCID 24193—
ProductHCID 135816406HCID 135816406—

Reaction Steps

In the same manner as in Example 1 and using ethyl 2-(2-aminoanilino)-6-methoxybenzo[b]thiophene-3-carboxylate, 1-methylpiperazine, anisole and titanium tetrachloride, 3-methoxy-12-(4-methylpiperazin-1-yl)-6H-[1]benzothieno[2,3-b][1,5]benzodiazepine is obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06271225B1
Source datasetuspto-grants-2001_08
ORD IDord-68199c2c501c4719af4c0d80d467f7a1
Source noteuspto-grants-2001_08