HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-2-nitrobenzene → HCID 18422279, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-2-nitrobenzene | HCID 6945 | — |
| Reactant | 221061-12-7 | HCID 18422225 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 18422279 | HCID 18422279 | 92.9% |
Reaction Steps
In the same manner as in Starting Material Synthesis Example 51 and using 2-amino-4-methylbenzo[b]thiophene-3-carbonitrile (3.8 g), 2-chloronitrobenzene(3.5 g) and dimethyl sulfoxide (45 ml), 4-methyl-2-(2-nitroanilino)benzo[b]thiophene-3-carbonitrile (5.8 g) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06271225B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-c6110a5ec63f41d3970338b0bb548167 |
| Source note | uspto-grants-2001_08 |