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HRID649948

反应详情

EQUATION

反应方程式

HRID 649948 的结构方程式

REACTANTS

反应物

2
结构：O=[N+]([O-])c1ccc(F)cc1F
HCID67967

1-Nitro-2,4-difluorobenzene

C6H3F2NO2

结构：N#Cc1c(N)sc2cc(F)ccc12
HCID18422184

2-Amino-6-fluoro-1-benzothiophene-3-carbonitrile

C9H5FN2S

PRODUCTS

生成物

1
结构：N#Cc1c(Nc2cc(F)ccc2[N+](=O)[O-])sc2cc(F)ccc12
HCID18422269

未命名化合物

收率 92.4%

PROCEDURE

实验过程

In the same manner as in Starting Material Synthesis Example 51 and using 2-amino-6-fluorobenzo[b]thiophene-3-carbonitrile (4.9 g) and 2,4-difluoro-nitrobenzene (4.1 g), 6-fluoro-2-(5-fluoro-2-nitroanilino)benzo[b]thiophene-3-carbonitrile (7.8 g) was obtained.

WORKUP

后处理

  1. customMaterial Synthesis Example 51