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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 649959Generated: October 30, 2026

1,1-Ethanedithiol → HCID 18422276, compound

https://huagongshe.com/reaction/649959

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,1-EthanedithiolHCID 33645—
ReactantAluminum(III) ChlorideHCID 6451240—
ReactantHCID 18422291HCID 18422291—
SolventDichloromethaneHCID 6344—
ProductHCID 18422276HCID 18422276—

Reaction Steps

In the same manner as in Example 62 and using 8-fluoro-10-methoxy-12-(4-methylpiperazin-1-yl)-6H-[1]benzothieno[2,3-b][1,5]benzodiazepine, dichloromethane, ethanedithiol and aluminium chloride, 8-fluoro-10-hydroxy-12-(4-methylpiperazin-1-yl)-6H-[1]benzothieno[2,3-b][1,5]benzodiazepine is obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06271225B1
Source datasetuspto-grants-2001_08
ORD IDord-1ba3d010a510462d97b054c56d062059
Source noteuspto-grants-2001_08