HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethylaniline → HCID 18422376, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethylaniline | HCID 949 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | Fumaric Acid | HCID 444972 | — |
| Reactant | HCID 18422160 | HCID 18422160 | — |
| Product | HCID 18422376 | HCID 18422376 | — |
Reaction Steps
In the same manner as in Example 80 and using 1,2,3,4-tetrahydro-[1]benzothieno[2,3-b][1,5]benzoxazepin-12(11H)-one (0.6 g), phosphorus oxychloride (5 ml), N,N-dimethylaniline (0.14 ml), 1-methylpiperazine (10 ml) and fumaric acid (260 mg), 1,2,3,4-tetrahydro-12-(4-methylpiperazin-1-yl)-[1]benzothieno[2,3-b][1,5]benzoxazepine fumarate (575 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06271225B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-e7f2d00dfde3419290477d8342f8da76 |
| Source note | uspto-grants-2001_08 |