2,2'-Azobis(2-methylpropanimidamide) dihydrochloride → HCID 86757238, compound

Participants

Reaction Conditions

Reaction Steps

N,N-diallyl 1,2,3,4-tetrahydroisoquinolinium bromide (15.0 g, EXAMPLE 5), and diallylammonium chloride (2.9 9, EXAMPLE 7) were dissolved in 18 mL deionized water. To this aqueous solution was added 0.5 g of 2,2′-azobis(2-amidinopropane) dihydrochloride, and the reaction mixture was bubbled with a slow stream of nitrogen gas for 45 minutes. While stirring, the temperature was raised to 70° C. The reaction mixture was stirred at 70° C. for 48 hours. After cooling to room temperature, 34.0 9 of viscous polymer solution was obtained.

Provenance & Evidence