HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl isocyanate → N-[4-(1-cyclopenten-1-yl)-1,3-dimethyl-1H-pyrazol-5-yl]-N'-phenylurea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl isocyanate | HCID 7672 | — |
| Reactant | 4-(1-cyclopenten-1-yl)-1,3-dimethyl-1H-pyrazol-5-amine | HCID 13352192 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | N-[4-(1-cyclopenten-1-yl)-1,3-dimethyl-1H-pyrazol-5-yl]-N'-phenylurea | HCID 13352208 | — |
Reaction Steps
Phenylisocyanate (0.176 mol) is added to 4-(1-cyclopenten-1-yl)-1,3-dimethyl-1H-pyrazol-5-amine (0.16 mol) in benzene (800 ml). The reaction mixture is stirred at room temperature and then at a temperature between 50° and 70° C. After distillation under vacuum, the product of the title is recovered by usual procedures. M.p. 204° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04612318 |
| Source dataset | uspto-grants-1986_09 |
| ORD ID | ord-8ae964ec380945738e640356bc097d75 |
| Source note | uspto-grants-1986_09 |