Decanoic Acid → HCID 86583986, compound

HRID 650463Notes

Reaction equation

[OH:1][C:2]([CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])=[O:3].[OH:13][CH2:14][C@@H:15]([C@H:17]([C@@H:19]([C@@H:21]([CH2:23][OH:24])[OH:22])[OH:20])[OH:18])[OH:16].C(O)(C)(C)C.[OH:30][C:31]([CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH3:41])=[O:32].OC[C@@H]([C@H]([C@@H]([C@@H](CO)O)O)O)O>O>[OH:3][C:2]([CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])=[O:1].[OH:32][C:31]([CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH3:41])=[O:30].[OH:24][CH2:23][C@@H:21]([C@H:19]([C@@H:17]([C@@H:15]([CH2:14][OH:13])[OH:16])[OH:18])[OH:20])[OH:22]

Participants

Conditions

Temperature: 35 °C

Procedure

A mixture of capric acid (0.86 g=5 mmole), sorbitol (ex Aldrich Chemical Co.) (0.91 g=5 mmole), t-butanol (500 μl), water (70 μl) and potato protein extract (100 mg) was stirred at 35° C. in a stoppered tube for 72 hours. Analysis of the resulting reaction mixture showed that sorbitol monocaprate (0.12 mmoles) and sorbitol dicaprate (0.04 mmoles) were formed.

Workup

extractionextract (100 mg)
customAnalysis of the resulting reaction mixture

Sources & evidence

ORD record: ord-00bf75164a5b43ebb941a5e47ccbd532
Source dataset: uspto-grants-2001_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06274357B1

Reaction notes

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