HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 11426171, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 5-Aminoisoquinoline | HCID 70766 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 11426171 | HCID 11426171 | — |
Reaction Steps
To a solution of 5-aminoisoquinoline (14.4 g, 100 mmol) in acetone (300 ml) was added iodomethane (14.4 ml). The solution was briefly stirred and then allowed to stand for 2 h. The yellow precipitate was then filtered, washed with acetone and dried to afford the title compound as a yellow solid (18.8 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06274594B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-03f83c946ffc443e83813e76deb81850 |
| Source note | uspto-grants-2001_08 |