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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 650685Generated: October 29, 2026

Imidazole → HCID 129689385, compound

https://huagongshe.com/reaction/650685

Reaction equation

Participants

RoleNameHCIDCharge
ReactantImidazoleHCID 795—
ReactantTetrafluoroboric acidHCID 28118—
SolventDiethyl EtherHCID 3283—
SolventDichloromethaneHCID 6344—
ProductHCID 129689385HCID 129689385—

Reaction Steps

To a solution of imidazole (20 mmol) in dichloromethane (30 mL) at 0° C. HBF4 (20 mmol, 3.8 g of a diethyl etherate) in dichloromethane is added dropwise. The reaction mixture is diluted with diethyl ether (100 mL) to precipitate the title compound. It is then filtered, washed with ether and recrystallized from ether.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06274725B1
Source datasetuspto-grants-2001_08
ORD IDord-a49c006aafe84e25ab8d16765c74025d
Source noteuspto-grants-2001_08